Dioxins & PCBs Purification Columns for Miura GO-xEHT Systems

The Miura GO-xEHT (GO-xHT) is a fully automatic sample preparation system for the analysis of Dioxins (DXNs) and Polychlorinated Biphenyls (PCBs), compounds considered Persistent Organic Pollutants (POPs). Find more details on this comprehensive Clean-up system here.

Features:

  • High performance clean-up
  • 4 columns
  • Heated purification and elution
    → better purification
    → faster elution
 
  • User-friendly design
  • Easy to apply sample
  • Easy connections
  • Disposable parts
    → no washing
    → no cross-contamination
  • Unique flow switching
  • Perfect separation of PCBs and Dixons in one freaction each
 Depending on the sample matrix and the analytes of interest, different column sets are available:

Composition of the Column Sets

(Standard setup)
 
Purification  
1 AgNO3 - Silica gel column
2 H2SO4 - Silica gel column
 
Concentration  
3 Carbon based column
4 Alumina based column (only needed for PCBs analysis)
 
 
 
Elution  
5 Dioxin Fraction
6 PCB Fraction
 
 
All columns and tubings needed are included in each set 
 

How it Works

  1. Dissolve the extracted sample in hexane and apply it to the column
    The system performs automatically the following steps
    - Clean-up
    - Concentration
    - Elution of PCBs fraction
    - Elution of Dioxins fraction
  2. Pick up the collected fractions
 
 

Column Sets and Recommended Applications

 
Sample type Environmental Samples  
  Food / Feed Samples
P/N 980-23882 980-22481 980-23881 980-26226
Type size [mm] DXNmini 18 Ø Standard 20 Ø Mini 18 Ø Hi-Capacity 20 Ø
Sample Environmental
- EPA -
Food 3 g fat
Environmental
Food 1 g fat
Environmental
Food up to 5 g fat
Purification (1) AgNO3-Silica gel AgNO3-Silica gel AgNO3-Silica gel H2SO4-Silica gel*
Purification (2) H2SO4-Silica gel H2SO4-Silica gel H2SO4-Silica gel KMnO4-Alumina*
AgNO3-Silica gel
Concentration (3) Carbon Carbon Carbon Carbon
Concentration (4) - Alumina Alumina Alumina
Solvent consumption
(Hexane)
85 ml 90 ml 85 ml 130 ml
DXN fraction (5)
(Toluene)
1.2 ml 1.2 ml 1.2 ml 1.2 ml
PCB fraction (6)
(Toluene)
- 1.0 ml 1.0 ml 1.0 ml
Run time 73 min 80 min 78 min 120 min
Each column set includes enough columns and tubings to perform 100 analysis 

*Reversed order of H2SO4- and AgNO3-Columns
 

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